IMEKO Event Proceedings Search

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J. Setina, J. Tesar, Z. Krajicek
Validation of a variable bell jar pressure as a method for primary generation of absolute pressure in the range from 100 Pa to 5 kPa

Generation of absolute pressure with a pressure balance is commonly done by enclosing the space above weights with a bell jar and evacuating it with a vacuum pump. Residual pressure in a bell jar is usually of the order of few tens of Pa to few Pa, depending on the effective pumping speed. Its value is added to a calculated pressure of the gravitational force of the piston and weights to obtain the generated absolute pressure. By connecting to the absolute pressure balance a precise and stable pressure gauge with sufficient resolution it is easy to observe that small changes of residual pressure in a bell jar generate a corresponding change in a pressure reading of the gauge. Unfortunately the lowest absolute pressure which can be generated by a pressure balance of conventional design is determined by the tare weight of the piston and some small additional weights necessary for sufficient minimum free rotation time and it is in the pressure range starting at 3 kPa and up to 5 kPa.

J. C. Torres-Guzmán, L. H. Paraguassú, P. R. G. Couto, I. L. Bezerra
SIM vacuum comparison from 133.3 Pa to 13.33 kPa

This comparison constitutes the second part of the first vacuum comparison among National Metrology Institutes (NMI) within the Interamerican Metrology System (SIM). Each laboratory used its national standards for the compared range. The Centro Nacional de Metrología (CENAM, Mexico) used a reference standard (comparison system type) and the Instituto Nacional de Metrologia, Normalização e Qualidade Industrial (INMETRO, Brazil) used a similar reference standard (comparison system type). The comparison started in December 2004 and finished in March 2005. The objective of the comparison was to estimate the level of agreement for the realization of the quantity and the uncertainty associated to its measurement.
One transducer (Capacitive Diaphragm Gauge) was used as transfer standard; the comparison range was selected from 133.3 Pa up to 13.33 kPa. The relevant aspects of the measurement protocol are summarized in the paper but were widely developed in the comparison reference documents. The gas used for the comparison was nitrogen. The measurements started at the lowest pressure and the pressure was increased up to the maximum range. The analysis of measurements comparability between the laboratories is included here. This bilateral comparison has been entered within the SIM data base as a pilot comparison SIM.7.26 P.

A. Navarro-Nateras, J. C. Torres-Guzman, P. Olvera-Arana
Measurement systems development for the calibration of leaks and holes in dynamic pressure (microflow) at CENAM, Mexico

The pressure and vacuum group of the Force and Pressure Division, at the Centro Nacional de Metrologia (CENAM, Mexico) has developed two measurement systems for calibration, one for leaks and another for holes in dynamic pressure.
The leaks calibration system is based on the method of pressure increment at constant volume (and constant temperature) within the measurement range starting at 1 x 10-6 Pa·m³·s-1 up to 5 Pa·m3·s-1 with volumes of 0.5 L or 1 L (according to the leak range to be calibrated), with an operation pressure from 1 x 10-5 Pa up to 130 kPa, using helium, nitrogen or air as manometric fluids.
For the calibration of holes in dynamic pressure, the method PVTt is used. This is, pressure increments at constant volume and constant temperature during a given time. The volume used is 3.75 L with a gas flow up to 20 cm³·min-1 using nitrogen as operation fluid.
The procedure of holes calibration consists on measuring the flow through a small hole by measuring the pressure increment due to the gas accumulation in a known volume during a period of time with controlled temperature conditions. The PVTt system is formed by pressure gauges, a gas collection tank with a known volume, temperature sensors, a chronometer for time measurement, a vacuum pump, a set of valves to control the gas flow direction and the hole which will be calibrated.

J. Galvan-Mancilla, J. C. Torres-Guzman, D. Ramirez-Ahedo
Torque proficiency test among accredited laboratories in Mexico

A torque proficiency test among accredited laboratories in Mexico was performed starting in January 2007. The main objectives of this exercise were to estimate the level of agreement for the dissemination of the quantity among laboratories and to evaluate the compatibility, including the uncertainty associated to its measurements, of the laboratories results with the set references values. The Centro Nacional de Metrologia, CENAM (Mexico) was the pilot laboratory and responsible for the coordination of this program. The maximum torque measurement for this proficiency test was 800 N·m. The torque standard TS used for the proficiency test was a torque wrench with a range up to 800 N·m. In this torque proficiency test 5 Mexican torque accredited laboratories participated. The results of the test showed good agreement among the laboratories and also with the reference values set by the national metrology institute (CENAM).

D. Ramirez-Ahedo, J. C. Torres-Guzman, F. Martinez-Juarez
Hybrid torque standard machine for 1 kN·m developed in CENAM

The torque laboratory at the Centro Nacional de Metrología in Mexico (CENAM) started operations in 1997 with the design, built up and set up of a torque transfer standard machine for 2 kN·m (TTSM-2kN·m). Since that time, a total of five torque standards have been developed at CENAM. Two of them realize the quantity via the primary method (dead weights applied in a lever arm of a well known length) in the measuring ranges of 2 kN·m and 1 kN·m. The other three transfer standard machines are in the ranges from 20 N·m and 2 kN·m, and the last one is a TTS machine which is in the set up stage, with a range up to 20 kN·m.
This paper gives general information about the design, build up and set up of the torque standard machine up to 1 kN·m which has a dual function, this is, realizing the quantity with a primary torque standard method (PTSMe) and/or disseminating it with a torque transfer standard method (TTSMe); depending on the type of calibration one wishes to perform.

S. Martínez-Sanchez, F. M. C. Laguna-Aguilar, J. C. Torres-Guzman
Metrology impact in Technological Universities, Mexico

The Universidades Tecnológicas (Technological Universities) in Mexico have as a mission to offer a high quality education model which has been in operation for more than 50 years in countries where it has proven to be a success. In 1998, the Centro Nacional de Metrología (CENAM) collaborated with the Technological Universities by means of an indepth technical training in Metrology. The objective was to disseminate the metrological knowledge among the academic members and stimulate them to establish secondary calibration laboratories in their institutions.

C. Ferrero
The intercomparison of Charpy impact pendulum calibration

The increasing demand, in particular in Italy, for calibration and certification work and for the accreditation of new calibration centres, is due to a number of concomitant factors: The need for industry to operate in accordance with EN 45000, ISO 9000 and ISO17025 as regards quality; the Italian law 273/91 establishing the National Calibration System, which comprises the Primary Metrological Institutes and the SIT centres).
INRiM provides for traceability to the standards of mechanical, thermal and electrical quantities all over the country, so as to allow high-quality measurements and tests to be made.
At present the number of SIT centres is 194 in total, plus 24 for force quantity (load cell, testing machines, impact pendulum, torque, extensometer).
One of the most important activities of the National Accreditation Body (NAB) is the organisation of a series of interlaboratory comparisons (ILC) to verify the best measurements capability of the accredited laboratories.
One of the difficulties in the technological field is represented by the big weight and large size of the equipments to calibrate, so it is difficult or impossible to circulate such equipments (e.g. materials testing machines or impact pendulum). In this case each participating Calibration Centre has to travel to the location were the equipment is located. Another difficulty for this kind of ILC is that the object of the comparison (the Charpy Impact Pendulum - CIP) has not the status of a reference standard. For this reason in 2005 one ILC was organised in Italy for the calibration of Charpy Impact Pendulum (CIP), with the following purposes:
1. to give an experimental validation of the resilience dissemination in Italy;
2. to evaluate the calibration competence of the different laboratories;
3. to give a contribution to solve the problem for future international comparison for such kind of equipments.
Two Charpy Impact Pendulum were chosen of 500 J and 20 J rated energy, located in one Calibration Centre.
At the experimental ILC participated 6 Calibration Centres, with a grand total of more than 50 first line standards. At each laboratory was asked to calibrate the CIP by using their normal procedure (usually UNI EN ISO 10045/2). The repeatability, accuracy and classification given by each lab were compared.
The main results of the metrological evaluation of the Charpy Impact Pendulum machines obtained during the ILC are discussed.

G. D’Agostino, A. Germak, C. Origlia, D. Quagliotti, G. Barbato
Measuring the free-fall acceleration with the IMGC-02 transportable absolute gravimeter

The knowledge of the acceleration g due to gravity plays an important role in force metrology in calibration of mechanical standards and, recently, in mass metrology in realizing new mass standards based on electrical references for the redefinition of kilogram. Moreover gravimetric surveys are carried on for applications in Geophysics and Geodesy.
Over the past thirty years the development of transportable ballistic absolute gravimeters has dramatically pushed up the ability to measure the g value. The application of new technological advances and the deep study of the physical phenomena influencing the gravity measurement allowed a significant reduction of the uncertainty, estimated to be some parts in 109. Nowadays the future progresses are expected to reduce instrumental size, weight, costs and operational simplicity.
The Istituto Nazionale di Ricerca Metrologica (INRIM) developed a transportable absolute gravimeter, called IMGC-02. It uses laser interferometry to measure, from an inertial reference point, the symmetrical free rise and falling motion of a test-body in the gravity field. The local g value is extracted from the trajectory by fitting a suitable motion model to the space-time coordinates.
The description of the instrument, the measurement principle, the reconstruction of the test-body trajectory, the user interface of the software and the results obtained during the last International Comparison of Absolute Gravimeters (ICAG-2005) are shown.

Antonio Cruz Serra, Leo Van Biesen
Aims, objectives, structure and activity of IMEKO - the instrumentation and measurement confederation

IMEKO is a non-governmental federation of 36 national Member Organisations. The Member Organisations are scientific/technical societies or committees. They include representatives of metrological institutions, higher education institutions, industry and users of instruments.
This communication will deal shortly with the objectives of the Confederation, will inform on its structure, will highlight IMEKO imeko_proceedings and will present an overview on the activities of the 23 Technical Committees.

Richard Davis
Recent advances on the redefinition of the kilogram

The International System of Units (SI) still relies on an artifact standard to define the unit of mass, the kilogram. The unit of electrical current, the ampere, is defined in terms of a force in newtons, which in turn is traceable to the kilogram. It has long been appreciated that the mass of any artifact, such as the international prototype of the kilogram, will certainly vary with respect to a so-called "fundamental" constant of mass, such as the mass of an atom of carbon-12. Until recently, however, there was no highly accurate experimental method that might link the mass of a macroscopic artifact to the mass of a fundamental constant. However, this situation is changing rapidly. Simultaneously with these developments, electrical metrology is now firmly based on fundamental constants, but these constants have rather large uncertainties due to the need to link the ampere to the kilogram in the present SI. Finally, in the field of fundamental constants, the need to measure certain of the constants in terms of the artifact kilogram in order to arrive at their SI values is becoming increasingly cumbersome. The present situation, as outlined above, has led to proposals to redefine a number of the SI base units.

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