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Thomas Fröhlich, Thomas Fehling, Benno Gatzemeier, Detlef Heydenbluth
SARTORIUS SUSCEPTOMETER FOR PRECISE MEASUREMENT OF SUSCEPTIBILITY AND MAGNETIZATION OF WEIGHTS

The Sartorius Susceptometer is a commercially available susceptometer as described in the Draft revision of International Recommendation OIML R111. It comes with a calibration sheet. The procedure of the factory calibration is described. A measurement comparing five calibrated susceptibility standards is discussed. The magnets used for calibration are monitored concerning the stability of the magnetic dipole moment over about one year.

K. Fukuda, K. Yoshida, T. Ono, K. Kameoka, T. Hirata
AN ADVANCED ALGORITHM FOR ESTIMATING AXLE WEIGHTS OF IN-MOTION VEHICLES

A signal processing method to improve the accuracy of measured axle weights of an in-motion vehicle is proposed and is evaluated by applying it to the actual weight signals from a new axle weighing system with a platform having a length of about 2.2m, approximately three times longer than that of a conventional one. In spite of several undesirable experimental conditions, the accuracy improvement was confirmed within the range of vehicle velocity, 5 ~ 40km/h.

Michael Kobusch, Thomas Bruns, Lioba Stenner, Sven-Patrick Schotte
IMPULSE FORCE INVESTIGATIONS OF STRAIN GAUGE SENSORS

This paper presents new investigations of strain gauge force sensors subject to impulse loads. Different approaches regarding the determination of the fundamental axial resonance are discussed in order to get information about a practical evaluation method for common-type strain gauge sensors under dynamic loads.

Sheau-shi Pan, H. C. Lu, C. S. Chang
INSTRUMENTS USED FOR MEASURING THE MAGNETIC PROPERTIES OF ONE KILOGRAM MASS STANDARD IN CENTER FOR MEASUREMENT STANDARDS (CMS)

We measured the volume magnetic susceptibility and permanent magnetization of 1 kg mass standards are measured under the circumstances of CMS mass laboratory. The method and calculation of uncertainty described here are referred to the experimental method and procedure developed by Davis; while the distance between magnetic sample and the weighs were measured with aluminium guide and the distance was determined by reading of laser interferometer. The effects of volume magnetic susceptibility and permanent magnetization on weights was real-time measured .The degree of real-time measured dependent upon the transient time of the balance. These results of susceptibility measurement were compared to the results of samples when they arrived CMS.

Chi Kah Lim, Bernd Glöckner, Thomas Allgeier
SHORT AND LONG-TERM BEHAVIOUR OF A 55 kN / 2.2 MN LEVER DEADWEIGHT FORCE STANDARD MACHINE

This paper describes the latest results from the re-verification of a 55 kN / 2.2 MN lever deadweight force standard machine at SPRING Singapore. For the first time, a lever machine was successfully compared against deadweight machines (from PTB) at the high level of 2 MN in both tension and compression with an uncertainty in the 1E-4 range. Similarly, the same applies to the 55 kN machine with an uncertainty of ±2E-5. For the 55 kN machine, both short-term and long-term uncertainty has been established. The machine had been the subject of an earlier comparison measurement with the PTB in the compression range. In addition, the periodic maintenance results of this 55 kN / 2.2 MN lever deadweight force standard machine will also be discussed. To monitor the drift and stability of the force realised, a total of 5 SPRING FTS were measured according to fixed protocols over time. The lever amplification ratio was also checked at intervals using a 50 kN FTS. From an earlier maintenance check, it was discovered that there was a significant drift in the lever ratio in March 2003 (12 months after commissioning). However, the deadweight forces continued to be realised within the ±2E-5 uncertainty. The lever ratio has since been adjusted back to producing loads which are magnified exactly 40 times from deadweight forces, demonstrating that it is capable of achieving ±1E-4 short term uncertainty. This was confirmed by the comparison with PTB up to 2 MN in both loading directions. Subsequent measurements demonstrated that the lever ratio has been stable. The same is also true for load reproducibility and repeatability at both the deadweight and lever machine, indicating that the long- term uncertainty is now satisfactory as well.

N.G. Domostroeva, A.V. Domostroev
PROBLEMS CRUDE OIL WEIGHT CALCULATION

This report describes problems of crude oil weight measurement in the tanks. The results of the crude oil density and temperature measurement are presented, obtained with the different method of sampling. The uncertainty budget in measuring the crude oil weight is given.

C. Ferrero, C. Marinari, E. Vilalta
APPLUS+ AND IMGC DEADWEIGHT FORCE MACHINES INTERCOMPARISON BY USING THE IMGC SIX-COMPONENT DYNAMOMETERS

Two IMGC multicomponent dynamometers were used to measure the parasitic components generated by the APPLUS+ 0,5 MN deadweight force standard machine. Results are presented which indicate that they are of a very low level. Measurements of the dynamic components during weight changes and free suspension of the system are also presented.

Bruno Andò, Pietro Giannone, Salvatore Graziani, Nicola Pitrone
MEASUREMENT SYSTEM FOR THE CHARACTERIZATION OF PIEZOELECTRIC BIMORPHS

Hysteresis is a common phenomenon in various non linear systems including piezoceramic materials. Piezoelectric bimorph devices show hysteretic behaviour, when operating as actuators. In this paper an experimental set-up to investigate the hysteretic behaviour of a PZT is described. The strategy adopted uses a resistive readout scheme and a CCD tool for the system calibration. Moreover, software tools have been developed to manage the experimental and to process signals coming from the hardware developed.

Michael Borys, Michael Gläser, Michael Mecke
MASS DETERMINATION OF SILICON SPHERES USED FOR THE AVOGADRO PROJECT

Spheres made of a silicon single crystal with a mass of about 1 kg are used as density standards and in the context of a project for the determination of the Avogadro constant. The status of the mass determination of such silicon spheres at the PTB is presented. Special facilities and procedures used for the mass determination in air are described. Results for a single sphere and the mass difference between two spheres are given with a discussion of the measurement uncertainty and mass stability.

Thomas Bruns, Michael Kobusch
DATA ACQUISITION AND PROCESSING FOR PTB'S IMPACT FORCE STANDARD MACHINE

The 20 kN Impact Force Standard Machine (IFSM) of PTB’s working group “Impact Dynamics” is supposed to provide traceability for dynamic force by measuring the acceleration of a steel body using a laser-Doppler-interferometer (LDI) [1]. The acceleration itself is derived from time dependant velocity data by numerical differentiation, which is a process prone to noise amplification. Therefore a thorough investigation of the data flow and data analysis algorithms concerning robustness, accuracy and the proliferation of disturbances is necessary. This paper describes the data acquisition system together with three different algorithms for digital demodulation of the LDI signal with regard to the boundary conditions given by the parameters of the equipment.

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