SIMPLIFIED EVALUATION OF THE SMALLEST SAMPLE MASS THAT SHOULD BE TAKEN FOR AN ACCURATE CHEMICAL ANALYSIS

Ricardo Rezende Zucchini
Abstract:
Technology has been developed very much during the last decades. In order to get better materials, with precise chemical composition, electrical properties, thermal properties, etc, it is a must to be capable to accomplish chemical analysis of blends, sometimes dealing with components in very low levels. Today, there are a number of new analytical techniques which allows quantifying extremely low levels of analytes, even employing very small samples. However, using small samples could generate sampling errors. Experimental determination of the minimum sample masses in order to get good accuracy can be a very costly operation, and a time demanding one. In this paper is proposed a simple method to evaluate the minimum sample mass that should be used in chemical analysis, to get low dispersion results.
Keywords:
Sampling, Sampling Constant, Precision, Particulate Matter
Download:
PWC-2006-TC10-011u.pdf
DOI:
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Event details
Event name:
XVIII IMEKO World Congress
Title:

Metrology for a Sustainable Development

Place:
Rio de Janeiro, BRAZIL
Time:
17 September 2006 - 22 September 2006